Structures by: Levason W.
Total: 678
[(AsBr3)2([16]aneSe4)]
[(AsBr3)2([16]aneSe4)]
Inorganic Chemistry (2002) 41, 2070-2076
a=10.12200(10)Å b=13.4494(2)Å c=10.5125(2)Å
α=90.0000(10)° β=113.49° γ=90.00°
C10H20AsCl3S4
C10H20AsCl3S4
Inorganic Chemistry (2002) 41, 2070-2076
a=13.5942(2)Å b=7.70070(10)Å c=18.1270(3)Å
α=90° β=111.1662(5)° γ=90°
C6H18Cl4P2Si
C6H18Cl4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=6.5363(3)Å b=8.2306(4)Å c=13.1544(8)Å
α=90.00° β=101.801(3)° γ=90.00°
C4H11ClP,Cl
C4H11ClP,Cl
Inorganic Chemistry (2013) 52, 5185-5193
a=12.000(6)Å b=10.204(5)Å c=12.936(6)Å
α=90.00° β=90.00° γ=90.00°
C6H18Br4P2Si
C6H18Br4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=14.408(5)Å b=8.465(3)Å c=13.448(5)Å
α=90.00° β=113.561(4)° γ=90.00°
C6H16Cl4P2Si
C6H16Cl4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=15.603(5)Å b=7.912(5)Å c=11.574(5)Å
α=90.000(5)° β=90.000(5)° γ=90.000(5)°
C6H16Br4P2Si
C6H16Br4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=11.285(3)Å b=11.285(3)Å c=23.543(10)Å
α=90.00° β=90.00° γ=90.00°
C10H24Br4P2Si
C10H24Br4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=9.353(3)Å b=11.954(4)Å c=17.285(6)Å
α=90.00° β=104.902(4)° γ=90.00°
C10H16Cl4P2Si
C10H16Cl4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=12.9646(4)Å b=15.2875(4)Å c=16.3211(12)Å
α=90.00° β=90.00° γ=90.00°
C10H28Cl4P4Si
C10H28Cl4P4Si
Inorganic Chemistry (2013) 52, 5185-5193
a=6.7173(10)Å b=8.6973(13)Å c=8.9154(13)Å
α=88.954(6)° β=89.753(6)° γ=86.672(7)°
Tetrabromo(1,2-bis(dimethylphosphanyl)benzene-P,P')silicon(IV) dichloromethane solvate
2(C10H16Br4P2Si),CH2Cl2
Inorganic Chemistry (2013) 52, 5185-5193
a=6.871(2)Å b=16.284(6)Å c=16.590(6)Å
α=90.00° β=101.940(4)° γ=90.00°
1,2-Bis(diethylphosphino)ethane-trichlorohydridosilicon(IV)
C10H25Cl3P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=9.209(6)Å b=11.870(7)Å c=15.399(11)Å
α=90.00° β=105.188(13)° γ=90.00°
Dichlorobis(1,2-bis(dimethylphosphino)benzene)gallium(III) tetrachlorogallate(III)
C20H32Cl2GaP41,Cl4Ga1
Inorganic chemistry (2007) 46, 17 7215-7223
a=13.2556(16)Å b=14.536(2)Å c=16.594(2)Å
α=90.00° β=104.131(8)° γ=90.00°
Dichloro(1,2-bis(diphenylphosphino)benzene)gallium(III) tetrachlorogallate(III)
C30H24Cl2GaP21,Cl4Ga1
Inorganic chemistry (2007) 46, 17 7215-7223
a=10.139(2)Å b=10.593(3)Å c=16.028(4)Å
α=72.765(12)° β=87.616(12)° γ=89.878(12)°
Dibromobis(1,2-bis(dimethylphosphino)benzene)gallium(III) tetrabromogallate(III) dichloromethane solvate
C20H32Br2GaP41,Br4Ga1,CH2Cl2
Inorganic chemistry (2007) 46, 17 7215-7223
a=14.688(3)Å b=22.978(4)Å c=10.4931(18)Å
α=90.00° β=90.00° γ=90.00°
1,2-bis(diethylphosphino)ethanebis(tri-iodogallium(III))
C10H24Ga2I6P2
Inorganic chemistry (2007) 46, 17 7215-7223
a=7.7763(18)Å b=7.818(2)Å c=10.993(3)Å
α=86.676(15)° β=82.577(15)° γ=80.447(18)°
Dichloro(1,2-bis(dimethylarsino)benzene)gallium(III) tetrachlorogallate(III)
C10H16As2Cl2Ga1,Cl4Ga1
Inorganic chemistry (2007) 46, 17 7215-7223
a=9.941(2)Å b=10.111(3)Å c=10.206(2)Å
α=90.00° β=91.303(16)° γ=90.00°
Di-iodo(1,2-bis(dimethylarsino)benzene)gallium(III) tetraiodogallate(III)
C10H16As2GaI21,GaI41
Inorganic chemistry (2007) 46, 17 7215-7223
a=15.935(4)Å b=11.374(2)Å c=14.319(3)Å
α=90.00° β=90.00° γ=90.00°
Bis(triiodogallium(III)){mu2-1,2-bis(diphenylarsino)ethane}
C26H24As2Ga2I6
Inorganic chemistry (2007) 46, 17 7215-7223
a=10.1666(10)Å b=15.4125(15)Å c=23.181(2)Å
α=90.00° β=99.036(5)° γ=90.00°
Tri-iodido(trimethylarsane)gallium(III)
C3H9AsGaI3
Inorganic chemistry (2007) 46, 17 7215-7223
a=7.103(2)Å b=11.444(4)Å c=8.076(3)Å
α=90.00° β=114.43(2)° γ=90.00°
Tribromido(trimethylarsane)gallium(III)
C3H9AsBr3Ga
Inorganic chemistry (2007) 46, 17 7215-7223
a=6.677(3)Å b=10.674(6)Å c=7.877(4)Å
α=90.00° β=113.57(3)° γ=90.00°
Diiodobis(1,2-bis(dimethylphosphino)benzene)gallium(III) tetraiodogallate(III) dichloromethane solvate
C20H32GaI2P41,GaI41,0.4(CH2Cl2)
Inorganic chemistry (2007) 46, 17 7215-7223
a=15.223(2)Å b=23.406(4)Å c=11.0027(10)Å
α=90.00° β=90.00° γ=90.00°
3(C6H11N2),Cl6Y
3(C6H11N2),Cl6Y
New J. Chem. (2016) 40, 8 7181
a=19.580(2)Å b=13.0359(15)Å c=11.1656(13)Å
α=90° β=90° γ=90°
C8H18Cl4MoS2
C8H18Cl4MoS2
Dalton transactions (Cambridge, England : 2003) (2018) 47, 7 2406-2414
a=8.6773(2)Å b=9.1092(2)Å c=19.7049(4)Å
α=90° β=98.465(2)° γ=90°
C34H28BiCl3O3P2
C34H28BiCl3O3P2
Journal of the Chemical Society, Dalton Transactions (2001) 7 1007
a=12.043(2)Å b=19.467(2)Å c=14.530(2)Å
α=90° β=101.80(2)° γ=90°
Tetracarbonyl(1,5-bis(dimethylstibino)-3-oxapentane)chromium(0)
C12H20CrO5Sb2
Dalton transactions (Cambridge, England : 2003) (2011) 40, 24 6565-6574
a=7.2837(5)Å b=13.933(2)Å c=17.804(3)Å
α=90.00° β=94.690(10)° γ=90.00°
(2,2'-bipyridyl)dichloridogermanium(ii)
C10H8Cl2GeN2
Dalton transactions (Cambridge, England : 2003) (2010) 39, 3 847-856
a=6.8277(5)Å b=17.957(3)Å c=9.0560(10)Å
α=90.00° β=94.057(10)° γ=90.00°
Trans-tetrachlorobis(methylselanylmethane-Se)tellurium(IV)
C4H12Cl4Se2Te
Dalton transactions (Cambridge, England : 2003) (2012) 41, 36 10988-10999
a=6.487(2)Å b=12.872(4)Å c=8.215(3)Å
α=90.00° β=108.245(8)° γ=90.00°
1,4,7,10,13,16-hexaoxacyclooctadecane-nitrato-lead(II) hexafluorophosphate
C12H24NO9Pb1,F6P1
Dalton transactions (Cambridge, England : 2003) (2013) 42, 13 4714-4724
a=12.958(5)Å b=8.475(3)Å c=9.296(3)Å
α=90.00° β=90.00° γ=90.00°
C6H16Cl2P2Sn
C6H16Cl2P2Sn
Dalton transactions (Cambridge, England : 2003) (2013) 42, 23 8364-8374
a=7.358(3)Å b=7.880(3)Å c=11.002(5)Å
α=74.68(2)° β=79.59(2)° γ=78.04(5)°
Catena-dibromo(2,6-dithiaheptane-S,S')selenium(II)
C5H12Br2S2Se
Dalton transactions (Cambridge, England : 2003) (2013) 42, 8 2963-2972
a=10.0866(16)Å b=8.0491(11)Å c=14.533(2)Å
α=90.00° β=109.211(8)° γ=90.00°
Diiodo(1,4,7-trioxa-10,13-dithiacyclopentadecane)calcium(ii)
C10H20CaI2O3S2
Dalton transactions (Cambridge, England : 2003) (2013) 42, 1 89-99
a=10.027(4)Å b=13.924(5)Å c=12.848(5)Å
α=90.00° β=101.82(4)° γ=90.00°
Catena-[(1,1,1-tris[(methylsulfanyl)methyl]ethane)-trichloroaluminium]
C16H36Al2Cl6S6
Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3637-3648
a=16.131(7)Å b=8.310(3)Å c=24.976(11)Å
α=90.00° β=107.156(8)° γ=90.00°
Trichlorobis(trimethylphosphine)aluminium(III)
C6H18AlCl3P2
Dalton transactions (Cambridge, England : 2003) (2014) 43, 39 14600-14611
a=9.970(3)Å b=10.599(4)Å c=13.562(4)Å
α=90.00° β=90.00° γ=90.00°
C30H22F4Ga2N6,P2F12,H8O4
C30H22F4Ga2N6,P2F12,H8O4
Dalton transactions (Cambridge, England : 2003) (2015) 44, 20 9569-9580
a=9.774(2)Å b=10.460(2)Å c=10.646(2)Å
α=78.064(12)° β=62.736(8)° γ=85.448(14)°
2(C32H12BF24),C16H24CaN8
2(C32H12BF24),C16H24CaN8
Dalton transactions (Cambridge, England : 2003) (2016) 45, 18 7900-7911
a=15.691(3)Å b=15.691(3)Å c=18.386(5)Å
α=90° β=90° γ=90°
C44H36BF24O4RbS2
C44H36BF24O4RbS2
Dalton transactions (Cambridge, England : 2003) (2015) 44, 43 18748-18759
a=13.923(3)Å b=16.765(3)Å c=22.402(5)Å
α=97.029(4)° β=105.185(5)° γ=90.376(3)°
Cis-tetrafluoro-bis(triphenylarsine oxide)zirconium(IV)
C36H30As2F4O2Zr,2(CH2Cl2)
Dalton transactions (Cambridge, England : 2003) (2012) 41, 40 12548-12557
a=15.175(5)Å b=16.254(6)Å c=16.340(6)Å
α=90.00° β=90.00° γ=90.00°
1,3-bis(2,6-Di-isopropylphenyl)imidazolium trimethyldichlorotin(IV)
C27H37N21,C3H9Cl2Sn1
Dalton transactions (Cambridge, England : 2003) (2012) 41, 40 12548-12557
a=9.801(2)Å b=20.775(5)Å c=15.552(4)Å
α=90.00° β=91.172(4)° γ=90.00°
Μ-oxido-bis[(tert-butylselenolato)bis(η^5^-cyclopentadienyl)niobium(IV)] toluene solvate
C28H38Nb2OSe2,C7H8
Acta Crystallographica Section C (2008) 64, 10 m321-m323
a=8.0288(10)Å b=12.7685(15)Å c=15.873(2)Å
α=90.00° β=92.848(6)° γ=90.00°
Bis(eta5-cyclopentadienyl)bis(methylselenolato)hafnium(IV)
C12H16HfSe2
Chemistry of Materials (2008) 20, 15 5100
a=9.5191(10)Å b=9.5191(10)Å c=14.604(2)Å
α=90.00° β=90.00° γ=90.00°
[bis[N-2-(dimethylstibanyl)benzyl]methanamine]- bis(dicarbonyl(cyclopentadienyl)iron(II)) tetrafluoroborate dichloromethane solvate
C33H37FeNO2Sb1,2(BF41),0.5(C1H2CL2)
Organometallics (2011) 30, 4 895
a=10.5977(10)Å b=11.799(2)Å c=16.732(3)Å
α=78.332(6)° β=86.814(8)° γ=85.261(8)°
Diiodo(1,2-bis(dimethylphosphino)benzene)indium(III) tetraiodoindate(III)
C10H16I2InP21,I4In1
Inorganic Chemistry (2008) 47, 9691-9700
a=16.322(3)Å b=11.2518(15)Å c=14.461(2)Å
α=90.00° β=90.00° γ=90.00°
Trans-dibromidobis(1,2-bis(dimethylphosphino)benzene)indium(III) tetrabromidoindate(III) dichloromethane solvate
C20H32Br2InP41,Br4In1,CH2Cl2
Inorganic Chemistry (2008) 47, 9691-9700
a=25.266(6)Å b=10.620(3)Å c=15.089(4)Å
α=90.00° β=113.129(10)° γ=90.00°
C10H24Cl4P2Si
C10H24Cl4P2Si
Inorganic Chemistry (2013) 52, 5185-5193
a=9.126(4)Å b=11.875(5)Å c=16.579(8)Å
α=90.00° β=104.159(7)° γ=90.00°
Bis(tribromogallium(III)){mu2-1,2-bis(diethylphosphino)ethane}
C10H24Br6Ga2P2
Inorganic chemistry (2007) 46, 17 7215-7223
a=7.4000(16)Å b=7.4685(16)Å c=10.805(2)Å
α=85.619(12)° β=88.087(12)° γ=77.456(12)°
Trichlorido(trimethylarsane)gallium(III)
C3H9AsCl3Ga
Inorganic chemistry (2007) 46, 17 7215-7223
a=6.443(2)Å b=10.168(4)Å c=7.776(3)Å
α=90.00° β=113.15(3)° γ=90.00°
[Pt{MeC(CH2SeMe)3}2][PF6]2
[Pt{MeC(CH2SeMe)3}2][PF6]2
Inorganic Chemistry (2000) 39, 3853-3859
a=12.272(9)Å b=18.563(9)Å c=15.285(7)Å
α=90° β=113.18(3)° γ=90°
[Ag{MeC(CH2SeMe)3}]CF3SO3
[Ag{MeC(CH2SeMe)3}]CF3SO3
Inorganic Chemistry (2000) 39, 3853-3859
a=8.120(2)Å b=15.374(3)Å c=14.071(2)Å
α=90° β=93.86(2)° γ=90°
[Ru{MeC(CH2SeMe)3}2][CF3SO3]2
[Ru{MeC(CH2SeMe)3}2][CF3SO3]2
Inorganic Chemistry (2000) 39, 3853-3859
a=8.658(3)Å b=11.533(3)Å c=8.659(2)Å
α=108.33(2)° β=91.53(3)° γ=106.01(2)°
Catena-(1,4,8,11-Tetrathiacyclotetradecane)trichlorogallium(III)
C10H20Cl3GaS4
Inorganic Chemistry (2012) 51, 2231-2240
a=21.781(4)Å b=6.5370(10)Å c=12.307(2)Å
α=90.00° β=108.560(10)° γ=90.00°
Dichloro(1,5,9,13-tetraselenacyclohexadecane)indium tetrachloroindate(III)
C12H24Cl2InSe41,Cl4In1
Inorganic Chemistry (2012) 51, 2231-2240
a=6.9436(15)Å b=22.508(5)Å c=8.4877(15)Å
α=90.00° β=100.735(10)° γ=90.00°
Dichloro(1,5,9,13-tetraselenacyclohexadecane)gallium tetrachlorogallate(III)
C12H24Cl2GaSe41,Cl4Ga1
Inorganic Chemistry (2012) 51, 2231-2240
a=9.9535(10)Å b=21.461(4)Å c=23.331(4)Å
α=90.00° β=90.00° γ=90.00°
1,1'-bi-1,5-diselenocan-1-ium bis(tetrachlorogallate(III))
C12H24Se42,2(Cl4Ga1)
Inorganic Chemistry (2012) 51, 2231-2240
a=9.0156(15)Å b=14.148(3)Å c=10.4855(15)Å
α=90.00° β=99.204(10)° γ=90.00°
1-chloro-1,5-diselenocan-1-ium tetrachlorogallate(III) dichloromethane solvate
C6H12ClSe21,Cl4Ga1,CH2Cl2
Inorganic Chemistry (2012) 51, 2231-2240
a=7.3566(10)Å b=12.521(2)Å c=18.670(3)Å
α=90.00° β=93.107(10)° γ=90.00°
(1,2-bis[(ethylthio)methyl]benzene)bis(trichlorogallium(III))
C12H18Cl6Ga2S2
Inorganic Chemistry (2012) 51, 2231-2240
a=18.561(4)Å b=10.809(3)Å c=13.495(3)Å
α=90.00° β=126.201(5)° γ=90.00°
1,2-phenylenebis[(chloromethyl)(methyl)sulfonium] bis(tetrachlorogallate(III))
C10H14Cl2S22,2(Cl4Ga1)
Inorganic Chemistry (2012) 51, 2231-2240
a=9.4813(15)Å b=14.009(3)Å c=18.403(3)Å
α=90.00° β=104.377(10)° γ=90.00°
Tris(1,2-bis(ethylthiomethyl)benzene)tetrakis(trichloroindium(III)) dichloromethane solvate
C36H54Cl12In4S6,2(CH2Cl2)
Inorganic Chemistry (2012) 51, 2231-2240
a=24.016(5)Å b=18.726(5)Å c=14.995(4)Å
α=90.00° β=114.76(2)° γ=90.00°
(bromodimethylstibine-Sb)dicarbonyl(cyclopentadienyl)iron(II) tetrafluoroborate
C9H11BrFeO2Sb1,BF41
Organometallics (2014) 33, 11 2693
a=8.8658(11)Å b=8.9344(12)Å c=9.3885(11)Å
α=107.836(8)° β=90.427(6)° γ=93.806(7)°
Bis-(bromodimethylstibine-Sb)carbonyl(cyclopentadienyl)iron(II) bromide
C10H17Br2FeOSb2,Br
Organometallics (2014) 33, 11 2693
a=7.2336(12)Å b=9.4231(12)Å c=25.906(7)Å
α=90.00° β=92.848(7)° γ=90.00°
Tetra(mu~2~-bromo)bis(N,N,N-tris[2-(dimethylstibanyl)benzyl]azane)- tetracopper(I)
C54H72Br4Cu4N2Sb6
Organometallics (2013) 32, 9 2760
a=17.908(6)Å b=14.592(4)Å c=26.275(9)Å
α=90.00° β=109.250(8)° γ=90.00°
Tricarbonyl-N,N,N-tris[2-(dimethylstibanyl)benzyl]azane-manganese(I) trifluoromethanesulfonate chloroform solvate toluene solvate
C30H36MnNO3Sb31,CF3O3S1,CHCl3,C7H8
Organometallics (2013) 32, 9 2760
a=16.758(4)Å b=14.392(3)Å c=19.233(7)Å
α=90.00° β=93.825(7)° γ=90.00°
Dicarbonyl-acetonitrile-N,N,N-tris[2-(dimethylstibanyl)benzyl]azane- manganese(I) trifluoromethanesulfonate diethyl ether solvate
C31H39MnN2O2Sb31,CF3O3S1,C4H10O
Organometallics (2013) 32, 9 2760
a=9.644(2)Å b=22.7495(12)Å c=19.7761(14)Å
α=90.00° β=102.835(11)° γ=90.00°
Tetra(mu~2~-bromo)bis(N,N,N-tris[2-(dimethylstibanyl)benzyl]azane)- tetracopper(I) dichloromethane solvate
C54H72Br4Cu4N2Sb6,4(C1H2Cl2)
Organometallics (2013) 32, 9 2760
a=11.755(3)Å b=12.875(4)Å c=13.094(5)Å
α=100.987(7)° β=93.589(7)° γ=101.211(7)°
6-[2-(dimethylstibanyl)benzyl]-12,12-dimethyl-5,6,7,12- tetrahydrodibenzo[c,f][1,5]azastibocin-12-ium iodide dichloromethane solvate
C25H30NSb21,I1,CH2Cl2
Organometallics (2013) 32, 9 2760
a=9.6461(13)Å b=11.2438(16)Å c=13.686(2)Å
α=102.791(7)° β=93.471(7)° γ=102.749(7)°
Di(mu~2~-bromo)bis(N,N,N-tris[2-(dimethylstibanyl)benzyl]azane)- tricopper(I) tetrafluoroborate dichloromethane solvate
C54H72Br2Cu3N2Sb61,BF41,1.5(CH2Cl2)
Organometallics (2013) 32, 9 2760
a=16.636(8)Å b=12.192(6)Å c=18.546(9)Å
α=90.00° β=104.656(8)° γ=90.00°
C10H24B2Br6P2
C10H24B2Br6P2
Inorganic chemistry (2016) 55, 17 8852-8864
a=11.412(7)Å b=7.255(4)Å c=14.002(9)Å
α=90.00° β=112.219(7)° γ=90.00°
C10H16BBr2P2,BBr4
C10H16BBr2P2,BBr4
Inorganic chemistry (2016) 55, 17 8852-8864
a=14.745(4)Å b=10.796(3)Å c=13.068(3)Å
α=90.00° β=90.00° γ=90.00°
C3H9BF3P
C3H9BF3P
Inorganic chemistry (2016) 55, 17 8852-8864
a=5.838(6)Å b=9.170(9)Å c=6.675(7)Å
α=90.00° β=113.359(11)° γ=90.00°
C25H22B1F2O2P21,B2F71
C25H22B1F2O2P21,B2F71
Inorganic chemistry (2016) 55, 17 8852-8864
a=10.446(4)Å b=10.871(4)Å c=12.470(5)Å
α=71.531(13)° β=86.113(14)° γ=85.936(15)°
C10H24B2F6P2
C10H24B2F6P2
Inorganic chemistry (2016) 55, 17 8852-8864
a=6.636(2)Å b=19.987(8)Å c=6.566(2)Å
α=90.00° β=108.286(9)° γ=90.00°
C10H24B2Cl6P2
C10H24B2Cl6P2
Inorganic chemistry (2016) 55, 17 8852-8864
a=11.138(6)Å b=6.934(4)Å c=13.505(8)Å
α=90.00° β=110.741(7)° γ=90.00°
C10H24B2I6P2
C10H24B2I6P2
Inorganic chemistry (2016) 55, 17 8852-8864
a=10.7029(19)Å b=11.820(2)Å c=19.582(4)Å
α=85.694(6)° β=85.145(6)° γ=77.051(5)°
C10H16BI2P2,I3
C10H16BI2P2,I3
Inorganic chemistry (2016) 55, 17 8852-8864
a=9.702(2)Å b=17.454(3)Å c=12.615(2)Å
α=90° β=97.751(4)° γ=90°
C12H32I3P4Sc
C12H32I3P4Sc
Inorganic chemistry (2016) 55, 24 12890-12896
a=13.902(2)Å b=13.902(2)Å c=25.589(8)Å
α=90.00° β=90.00° γ=90.00°
C20H32I3P4Sc
C20H32I3P4Sc
Inorganic chemistry (2016) 55, 24 12890-12896
a=8.8820(10)Å b=8.8820(10)Å c=35.4690(10)Å
α=90.00° β=90.00° γ=90.00°
C16H32NaS8,C32H12BF24
C16H32NaS8,C32H12BF24
Inorganic chemistry (2015) 54, 6 2497-2499
a=12.8461(16)Å b=12.9256(17)Å c=18.696(2)Å
α=80.074(5)° β=72.780(4)° γ=89.917(6)°
C14H28NaO2S3,C32H12BF24
C14H28NaO2S3,C32H12BF24
Inorganic chemistry (2015) 54, 6 2497-2499
a=12.3957(17)Å b=12.4121(17)Å c=19.061(3)Å
α=102.501(5)° β=102.215(6)° γ=92.001(4)°